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The research included the preparation of the New Azo Schiff Ligand derived from 4,5-diphenyl imidazole. The ligand was prepared from the amine reactor with the coupling component in order to prepare the azo amino benzayl amine. After that the last compound and vinilline which obtained the ligand mentioned some metallic complexes were prepared for the ions of Cu(II), Zn(II) and Cd(II). The New azo- Schiff ligand complexes after purification were identification by using the available spectral and analytical methods such as Mass spectrum for the New ligand and (ultraviolet- visible, FTIR) spectroscopy, CHN analytics', Atomic absorption, and conductivity measurement. According to these techniques the New Azo – Schiff ligand was pidentate and the proposed geometrical shape was octahedral for the three complexes.